Acessibilidade / Reportar erro

Evaluation of microstructure and magnetic properties of copper ferrite doped with lead sintered with liquid phase

ABSTRACT

This paper presents to obtain a lead and copper ferrite with spinel structure, characterizing the microstructure and the determination of their magnetic properties. The copper and lead ferrite is a material with low magnetic coercivity, high electrical resistivity. Samples with stoichiometry PbxCu1-xFe2O4 with (x = 0.00; 0.05; 0.10; 0.15 e 0.20) were prepared by powder metallurgy processes and sintered at 1000 °C for 6 hours. The results show that sample with x = 0.00 is formed exclusively by the cubic spinel structure and samples with x between 0.05 to 0.20 are formed exclusively by the tetragonal spinel structure hysteresis loops show the characteristics of a soft magnetic material and the saturation magnetization and Curie temperature decreased with the lead concentration, however, noted that the increase in the coercive field.

Keywords:
Lead ferrites; Microestruture; Liquid Phase; Magnetic properties; Jahn-Teller Effect

Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro, em cooperação com a Associação Brasileira do Hidrogênio, ABH2 Av. Moniz Aragão, 207, 21941-594, Rio de Janeiro, RJ, Brasil, Tel: +55 (21) 3938-8791 - Rio de Janeiro - RJ - Brazil
E-mail: revmateria@gmail.com